Table 2.

Guest contents determined by 1H NMR spectroscopy and GC.

guest/TMP ratio
guest1H NMR (methyl)1H NMR (aryl)13C CP-MAS NMRGCTGA
toluene0.680.65guest observed1.600.40
o-xylene0.440.42a1.970.46
m-xylene0.160.15a0.850.46
p-xylene0.220.21guest observed0.380.24
tetramethylbenzene0.160.12guest observedaa
tetrafluorobenzene0.24n.a.guest observed0.32a
pentaneaaa0.00a
cyclohexane00a0.01a
perfluoro(methylcyclohexane)00a0.00a
  • aNo measurement made.